PROCESS MONITORING AND PROCESSING FACILITIES


Technique Type of apparatus
Partner name, Contact person
Expertise of the personel
Types of possible experiments
Compounding / Extrusion
Extruders
Feeding equipment
Downstream equipment
Monitoring
Injection moulding
Further equipments and tests
IPF
Kretzschmar, Bernd
Tel.: +49(0)3514658-338


Dipl.-Phys. , Head of the Processing Laboratory
-Physical and reactive compounding of thermoplastics, e.g. polymeric nanocomposites, biologically degradable materials, flame-retardant polymers, blends
-Extrusion monitoring, e.g. on-line analysis (NIR, ATR, Raman, ultrasonics) and on-line morphology analysis (particle sizes, particle size distributions)
- Compounding/Extrusion

- Injection moulding

- Tests: Flammability tests; Testing equipment related to processing stages;

- Simulation of ageing
Extrusion
Extruder : Krupp Werner&Pfleiderer
SICOMP
Lars Liljenfeldt,
Marketing manager
Tel.: +46 (0) 911 744 40

- Compounding of natural fibre as wood, flex, hemp together with thermoplastics
Process laboratory with scale manufacturing equipment for experiments, prototype manufacturing and testing:
Filament winding
Waltritsch & Wachter
SICOMP
Lars Liljenfeldt,

Marketing manager
Tel.:+46 (0) 911 744 40

- Process development and process optimization with respect to filament winding
Process laboratory with scale manufacturing equipment for experiments, prototype manufacturing and testing:
Cutting machine
GerberGTxL
SICOMP
Lars Liljenfeldt,

Marketing manager
Tel.:+46 (0) 911 744 40

- Optimization of cutting pattern and delivery of pre-cut reinforcement
Process laboratory with scale manufacturing equipment for experiments, prototype manufacturing and testing:
Press
Fjellman 310 ton press force
SICOMP
Lars Liljenfeldt,

Marketing manager
Tel.:+46 (0) 911 744 40

- Process development and process optimization with respect to compression moulding of SMC and GMT
Process laboratory with scale manufacturing equipment for experiments, prototype manufacturing and testing:
Infusion equipment
Mould carrier, equipment and facilities for RTM and vacuum infusion
SICOMP
Lars Liljenfeldt,

Marketing manager
Tel.:+46 (0) 911 744 40

- Process development and process optimization with respect to infusion technologies
Process laboratory with scale manufacturing equipment for experiments, prototype manufacturing and testing:
Automatization
ABB robot
SICOMP
Lars Liljenfeldt,

Marketing manager
Tel.:+46 (0) 911 744 40

- Development of robot cells and automatization of product manufacturing
Extrusion
Twin Screw Extruder mod. MD30-19/A
Bausano e Figli S.p.A.
INSTM
Prof. J.M. Kenny

Processing of polymeric materials.
-Extrusion of pure thermoplastic polymers.
-Melt blending of thermoplastic polymers.
-Melt blending of thermoplastic polymers and inorganic additives (i.e. microcomposites, nanocomposites).
Flammability test (UL94)
Flammability test (UL94), Oxygen index (ASTM D2863-00), Ash evaluation (UNI EN ISO 3451 - method a)
Cone calorimeter tests (ISO 5660) - 3 specimens
INSTM
Prof. J.M. Kenny

Evaluation of fire resistance of polymers and nanocomposites
Injection Moulding
Sandretto Micro 30/107
Sandretto Industrie SPS
INSTM
Prof. J.M. Kenny

Sample production;Investigation on the material performance (mechanical properties, weight, density, ecc.) for different processing parameters.
Resin Transfer Moulding
Hypaject MkII
Plastech Thermoset Tectonics
INSTM
Prof. J.M. Kenny

-Sample production
- Investigation and Modelling on the permeability and the Capillary pressure of the fibrous reinforcement;
- Flow models verification (flow front evolution, flow rate, pressure profiles and pressure loss  inside the cavity)
QUV Accelerated weathering Tester
QUV/spray
Solar eye - spray, UVB lamps - Tensile Adaptor Panel Holder
INSTM
Prof. J.M. Kenny

Materials can be subjected to artificial and accelerated weathering tests which simulate natural weathering. Controlled cycles of ultraviolet radiation, water spray, and heating elements are used to simulate the natural conditions of sun, rain and temperature changes.
Plasma (MPA/CVD) equipment

INSTM
Prof. J.M. Kenny

Carbon film deposition and surface treatments, spin coating and thermal evaporator for thin film deposition.
Microdielectrometry for in situ monitoring

Dielectric Spectrometer
Micromet and Netzch

UCBL
Dr.Gérard Seytre


In situ-monitoring of chemical and physical events

-Curing of thermoset and coating, phase separation, cristallisation, monitoring of chemical events
In line UV/Fluorescence for extrusion processing
PVT-100,Home made
UCBL
Prof.Cassagnau


-Reactive extrusion
-Mixing and dispersion in molten polymers.

- In line measurement of the residence time distribution in continuous processing machines. Mixing characterization
TGA/GC/MS
Coupled techniques between thermal gravimetric analysis, gas chromatography and mass spectroscopy, Setaram
UCBL
Dr. Bounor-Legaré


-Reactive extrusion
-Chemical modification of polymers in molten condition

- Polymer degradation
Quantification of reaction sub products for reactive processing application
Organic volatile compounds

Rubber Processing Analysis Rubber Processing Analyser, RPA
CSIC
Dr. Miguel Angel Lopez Manchado

Processing and characterization of rubber compounds: Preparation of compounds, vulcanization reaction, cure kinetics, mechanical, dynamical and thermal properties
The properties of raw rubber, compounded or product for cure time, strain sweep, frequency sweep, temperature sweep, matrix, stress relaxation, variable temperature analysis and delay.
Biological laboratory
microbiology, toxicology, flow cytometry, spectrophotometry,spectrofluorometry, Fluorescence Microscopy).
TECNALIA
Tribological tests: wear and friction.
Measurement of topography: roughness meter, non-contact profilometry, AFM, etc. Coatingtests (Adherence, conventional hardness, ultramicrohardness, thickness, crystallinity, composition and microstructure, etc.). Microhardness tests (Vickers and Knoop). Measurement of hydrophobicity (surface energy): Angle of contact.
Flammability test (UL94) Vertical burning test: UL 94,
cone calorimeter: ISO 5660 and Smoke density: ISO 5659-2,
Oxygen index test (LOI)
TECNALIA,
Dr. Aitor Barrio
Characterization and research on flame retardant additives behaviour dispersed in different
polymers
Production of polymeric composite materials
Semi industrial Autoclave,Aeroform, UK
FORTH
Prof.Costas Galiotis

Tel.: +30 2610965300

Production of :
-composites incorporating shape memory alloys
-polymeric composites
-nanocomposites using the RFI technique
-different types of polymeric composites with different reinforcing fibers
-Polymer curing and Post curing
-Production of composites by vacuum bagging of material in prepared form
-Production of nanocomposites with Resin Film Infusion
-Monitoring of curing process with different types of sensors
Zone-Casting Zone-casting layer deposition system TUL
Dr. Ireneusz Glowacki


Dr. Beata Luszczynska


Dr. Jaroslaw Jung

Tel.: +48 426313205
- Producing of the high oriented layers using the low molecular weight materials with the tendency to crystallization
Spin-coating Spin 150 (apparatus adapted to work in oxygen-free environment);
3LE Laboratory Equipment GmbH Delta 10
TUL
Dr. Ireneusz Glowacki


Dr. Beata Luszczynska


Dr. Jaroslaw Jung

Tel.: +48 426313205
Producing of thin layers using organic low molecular weigh materials and polymers

Oxygen-free environment.
Multi-step program
with the ability to set different times and rotation speed;
Metal layers evaporation Evaporator MK11- evaporation of metallic layers
- Multilayer evaporation (changing the source of  evaporated metal)


TUL
Dr. Ireneusz Glowacki


Dr. Beata Luszczynska


Dr. Jaroslaw Jung

Tel.: +48 426313205
- work in oxygen-free environment(Evaporator MK11):
- Evaporation from 4 sources
- possibility to change of inclination angle between plane of a sample and immobile evaporated metal source
- ability to rotate evaporated sample
(apparatus adapted to work in oxygen-free environment);
Evaporator Edwords 306 Turbo
Producing of  optoelectronic devices like
OFET, OLED, OPV in oxygen-free conditions
Stand in oxygen-free conditions includes:
magnetic stirrer ”IKA RCT Basic safety control”;
„Glass ceramic Hot Plate CT10”;
analytical balance ”cole paramer PA-120 Symmetry”;
spin-coater,
vacuum dryer;
stand dedicated for device
encapsulation; 
welding machine;
TUL
Dr. Ireneusz Glowacki


Dr. Beata Luszczynska


Dr. Jaroslaw Jung

Tel.: +48 426313205
- Producing of optoelectronic devices like OFET, OLED, OPV with using spin-coating and drop-casting techniques

-drying prepared samples in vacuum dryer

- encapsulation and protection of samples from external conditions during transport
Plasma system
Plasma system Atto (Diener Electronic)

TUL
Dr Ireneusz Glowacki

Tel.: +48 426313205
- Process development, surface cleaning, activating, etching


 

stat4u